Method of presenting of results in qualitative analysis
Experiment |
Observation |
Conclusion |
||||
Put one spatula endful of the sample in a dry test tube and heat. |
On gentle heating, water condensed on cooler parts of test tube a colour with pungent smell, was gas evolved. It turns red litmus blue and fumed HCI(g). Colourless gas with a chok adour evolved which turns blue decolourises potassium permanganate red-brown residue after heating. |
|
||||
Put one spatula endful of the sample in a test tube and add water. |
The solid dissolves forming a pale green solution. |
Probably Fe2+, CU2+, Ni2+ present. |
||||
To the aqueous solution in a test tube add NaOH(aq) dropwise until in excess |
Dirty green precipitate insoluble in excess, turns brown on exposure to air. On warming, a colour-less gas, with 000000a pungent smell was evolved, it turned red litmus blue and .. |
|
||||
To 1cm3 of the solution in a test tube, add aqueous ammonia dropwise until in excess |
Dirty green precipitate insoluble in excess, turned brown on exposure to air. |
|
||||
To 1cm3 of the solution in a test tube, add dil. HNO33)2(aq) followed by Ba(NO |
White precipitate, insoluble in the acid |
|
||||
To 1cm3 of the test tube, add potassium
|
Dark blue precipitate |
|
||||
To 1cm3 of the solution in the test tube, add AgNO3(aq) |
White precipitate |
|
Identify the;
|
Fe2+ and NH4
|
|
Zn(OH)2(s) + 4NH3(aq) Zn(NH3) 4(aq) - 2OH-(aq)